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 20.11.2009   Карта сайта     Language По-русски По-английски
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20.11.2009

Solvothermal synthesis, nanocrystal print and photoelectrochemical properties of CuInS2 thin film



Fei Longa, b, Corresponding Author Contact Information, E-mail The Corresponding Author, Wei-Min Wanga, Hua-chao Taob, Tie-kun Jiaa, Xiao-Min Lib, Zheng-guang Zoub and Zheng-yi Fua






aState Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan 430070, China


bKey Laboratory of New Processing Technology for Nonferrous Metals and Materials, Ministry of Education, Guilin University of Technology, Guilin 541004, China






Received 27 August 2009; 


accepted 20 October 2009. 


Available online 24 October 2009.






Abstract


CuInS2 nanoflakes were synthesized successfully by a convenient solvothermal route in ethylene glycol under the open-air condition using copper chloride, indium chloride and thiourea as starting materials. The factors which might affect the purity of the product during the synthesis were discussed. It's found that the products were significantly affected by the reaction time, temperature and the diffusion of the reactors. CuInS2 nanoflakes ink was prepared and coated onto Mo substrate using blade technology, and after sintering, a dense and compact CuInS2 film was produced. The morphological of the precursor films and CuInS2 films were done by scanning electron microscope (SEM), and the photoelectrochemical properties and morphology of the CuInS2 thin film were characterized.





Keywords: CuInS2; Nanomaterials; Solar energy materials; Solvothermal synthesis





Article Outline



1. Introduction
2. Experimental details

2.1. Preparation of CuInS2 nanoflakes
2.2. Production of the CuInS2 thin film
2.3. Characterization of the CuInS2 thin films

3. Results and discussion
4. Conclusion
Acknowledgements
References




























Corresponding Author Contact InformationCorresponding author. State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan 430070, China. Tel.: +86 773 5896700; fax: +86 773 5896671.










Materials Letters
Volume 64, Issue 2, 31 January 2010, Pages 195-198


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  • Chen Wev .  honorary member of ISSC science council

  • Harton Vladislav Vadim  honorary member of ISSC science council

  • Lichtenstain Alexandr Iosif  honorary member of ISSC science council

  • Novikov Dimirtii Leonid  honorary member of ISSC science council

  • Yakushev Mikhail Vasilii  honorary member of ISSC science council

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